Formal [2+2] Cycloaddition of 2-Acylaminoacrylates with Vinyl Sulfides. An Approach to Cyclobutane-alfa-Amino Acids as S-Phenylcysteine Analogues
- Avenoza, A. 1
- Busto, J.H. 1
- Mata, L. 1
- Peregrina, J.M. 1
- Pérez-Fernández, M. 1
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1
Universidad de La Rioja
info
ISSN: 0039-7881
Argitalpen urtea: 2008
Alea: 5
Orrialdeak: 743-746
Mota: Artikulua
Beste argitalpen batzuk: Synthesis (Stuttgart)
Laburpena
Two new types of conformationally restricted S-phenylcysteine are presented. The restriction comprises a cyclobutane unit that includes the α- and β-carbons of the α-amino acid. The synthetic strategy is based on a formal [2+2] cycloaddition between 2-(acylamino)acrylates as acceptor alkenes and vinyl sulfides as donor alkenes, promoted by aluminum-derived bulky Lewis acids. © Georg Thieme Verlag Stuttgart.